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| Авторы: | Gismatulina Yu.A., Budaeva V.V., Sakovich G.V. |
| Название публикации: | Nitrocellulose Synthesis from Miscanthus Cellulose |
| Название источника: | Propellants, Explosives, Pyrotechnics |
| Библиографическая ссылка: | Gismatulina Yu.A., Budaeva V.V., Sakovich G.V. Nitrocellulose Synthesis from Miscanthus Cellulose // Propellants, Explosives, Pyrotechnics. - 2018. - Vol.43. - Iss.1. - P.96-100. |
| Библиографическая ссылка2: | Y. A. Gismatulina, V. V. Budaeva, G. V. Sakovich, Prop., Explos., Pyrotech. 2018, 43, 96. |
| Ссылки: | DOI: 10.1002/prep.201700210; WoS: 000419977300013; SCOPUS: 2-s2.0-85031669101; РИНЦ: 35525666; |
| Реферат: | The possibility of synthesizing nitrocellulose (NC) from an easily renewable non‐woody feedstock, Miscanthus, is demonstrated herein. Nitration of Miscanthus cellulose with commercial mixed acid was found to afford high‐quality NC: 11.85 % nitrogen content, 18 cP viscosity of 2 % NC‐acetone solution, 97 % solubility in alcohol‐ester mixture, and 0.11 % ash content. The Miscanthus NC structure and fibers were characterized by analytical techniques such as SEM, IR spectroscopy, TGA/DTG, and 13C NMR spectroscopy. The Miscanthus NC is comparable in quality to basic NC types used for the manufacture of films, membranes, lacquers, nail polish, liquid bandage, artificial silk and skin. |
| Ключевые слова: | Miscanthus, cellulose nitrate, SEM, TGA/DTG, IR spectroscopy |
| Год опуликования: | 2018 |